Abstract
This paper investigated the encapsulation complex (EC) of chlorine dioxide (ClO2) in α-cyclodextrin. The encapsulation process was evaluated with varying molar ratios of ClO2 to α-cyclodextrin; the structure of the EC was characterized using FTIR, XRD, and microscopy imaging; and the release and retention of ClO2 was measured using UV–vis spectrophotometry. Results showed that high ClO2 loading and EC yield were achieved using appropriate ClO2/α-cyclodextrin ratio. Characterization analyses showed that α-cyclodextrin was oxidized by ClO2 and agglomerated into larger particles with modified crystallinity. The retention of ClO2 at −20 °C was stable for at least 3 months. The release of ClO2 followed an anomalous transport process in which diffusion played an important role. The release rate was relatively slow compared to some ClO2 releasing systems reported in the literature, suggesting this EC had potential for applications requiring an extended releasing period.
| Original language | English (US) |
|---|---|
| Article number | 106783 |
| Journal | Food Control |
| Volume | 107 |
| DOIs | |
| State | Published - Jan 2020 |
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All Science Journal Classification (ASJC) codes
- Biotechnology
- Food Science
Keywords
- Chlorine dioxide
- Controlled release
- Structure characterization
- α-cyclodextrin
Cite this
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Encapsulation complex of chlorine dioxide in α-cyclodextrin : Structure characterization and release property. / Chen, Mo; Chen, Xi; Yam, Kit.
In: Food Control, Vol. 107, 106783, 01.2020.Research output: Contribution to journal › Article
TY - JOUR
T1 - Encapsulation complex of chlorine dioxide in α-cyclodextrin
T2 - Structure characterization and release property
AU - Chen, Mo
AU - Chen, Xi
AU - Yam, Kit
PY - 2020/1
Y1 - 2020/1
N2 - This paper investigated the encapsulation complex (EC) of chlorine dioxide (ClO2) in α-cyclodextrin. The encapsulation process was evaluated with varying molar ratios of ClO2 to α-cyclodextrin; the structure of the EC was characterized using FTIR, XRD, and microscopy imaging; and the release and retention of ClO2 was measured using UV–vis spectrophotometry. Results showed that high ClO2 loading and EC yield were achieved using appropriate ClO2/α-cyclodextrin ratio. Characterization analyses showed that α-cyclodextrin was oxidized by ClO2 and agglomerated into larger particles with modified crystallinity. The retention of ClO2 at −20 °C was stable for at least 3 months. The release of ClO2 followed an anomalous transport process in which diffusion played an important role. The release rate was relatively slow compared to some ClO2 releasing systems reported in the literature, suggesting this EC had potential for applications requiring an extended releasing period.
AB - This paper investigated the encapsulation complex (EC) of chlorine dioxide (ClO2) in α-cyclodextrin. The encapsulation process was evaluated with varying molar ratios of ClO2 to α-cyclodextrin; the structure of the EC was characterized using FTIR, XRD, and microscopy imaging; and the release and retention of ClO2 was measured using UV–vis spectrophotometry. Results showed that high ClO2 loading and EC yield were achieved using appropriate ClO2/α-cyclodextrin ratio. Characterization analyses showed that α-cyclodextrin was oxidized by ClO2 and agglomerated into larger particles with modified crystallinity. The retention of ClO2 at −20 °C was stable for at least 3 months. The release of ClO2 followed an anomalous transport process in which diffusion played an important role. The release rate was relatively slow compared to some ClO2 releasing systems reported in the literature, suggesting this EC had potential for applications requiring an extended releasing period.
KW - Chlorine dioxide
KW - Controlled release
KW - Structure characterization
KW - α-cyclodextrin
UR - http://www.scopus.com/inward/record.url?scp=85069867907&partnerID=8YFLogxK
UR - http://www.scopus.com/inward/citedby.url?scp=85069867907&partnerID=8YFLogxK
U2 - 10.1016/j.foodcont.2019.106783
DO - 10.1016/j.foodcont.2019.106783
M3 - Article
AN - SCOPUS:85069867907
VL - 107
JO - Food Control
JF - Food Control
SN - 0956-7135
M1 - 106783
ER -