Solvothermal synthesis of acmite conversion coatings on steel

Terence Whalen, Bryan Vansaders, Cekdar Vakifahmetoglu, Asad Mughal, Eugene Zlotnikov, Seung Beom Cho, Richard Riman

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Abstract

Acmite (NaFeSi2O6) films were formed on steel coupons via solvothermal reaction of silica, sodium hydroxide, and 1, 4-butanediol in an autoclave under autogenous pressure. Systematic variation in processing variables led to homogenous coatings comprised of pinacoidal acmite grains with an average grain size of ~33 μm. The coatings were produced on the steel coupons from reactant conditions of 0.635 m SiO2, 2.546 m NaOH, and 3.087 m 1,4-butanediol for 72 h at 240°C.

Original languageEnglish (US)
Pages (from-to)3656-3661
Number of pages6
JournalJournal of the American Ceramic Society
Volume96
Issue number11
DOIs
Publication statusPublished - Nov 1 2013

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All Science Journal Classification (ASJC) codes

  • Ceramics and Composites
  • Materials Chemistry

Cite this

Whalen, T., Vansaders, B., Vakifahmetoglu, C., Mughal, A., Zlotnikov, E., Cho, S. B., & Riman, R. (2013). Solvothermal synthesis of acmite conversion coatings on steel. Journal of the American Ceramic Society, 96(11), 3656-3661. https://doi.org/10.1111/jace.12594