Synthesis of (–)-Methyl Ravidosaminide

Spencer Knapp, G. Sankar Lai, Divya Sahai

Research output: Contribution to journalArticlepeer-review

28 Scopus citations

Abstract

The title compound (9b) was prepared in five steps (48% overall yield) from ethyl 2,3,6-trideoxy-α-D-erythro-hex-2-enopyranoside (4b) as a 1:2.3 mixture of a- and /3-anomers. The key step was the iodocyclization reaction of unsaturated carbonimidothioate derivative 5. An improved procedure for the synthesis of 4b is also described.

Original languageEnglish (US)
Pages (from-to)380-383
Number of pages4
JournalJournal of Organic Chemistry
Volume51
Issue number3
DOIs
StatePublished - 1986

All Science Journal Classification (ASJC) codes

  • Organic Chemistry

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